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TCE Chemistry — Level 4

Redox Titration — Flashcards & Quiz

Redox titration determines the concentration of an oxidising or reducing agent by titrating against a standard of known concentration. TCE Chemistry Level 4 commonly uses permanganate (MnO₄⁻) or dichromate (Cr₂O₇²⁻) as the oxidising titrant, and asks you to balance the half-equations, combine them for the net ionic equation, and calculate the unknown concentration from the titre.

Key Points

  • Permanganate (MnO₄⁻) in acidic solution reduces to Mn²⁺: MnO₄⁻ + 8H⁺ + 5e⁻ → Mn²⁺ + 4H₂O.
  • Dichromate (Cr₂O₇²⁻) in acidic solution reduces to Cr³⁺: Cr₂O₇²⁻ + 14H⁺ + 6e⁻ → 2Cr³⁺ + 7H₂O.
  • Permanganate is self-indicating — the endpoint is marked by a persistent pink colour when excess MnO₄⁻ is added.
  • Dichromate needs an indicator (e.g. diphenylamine sulfonate) because the colour change is less obvious.
  • Balancing: balance atoms first, then charges with electrons, then combine half-equations to cancel electrons.
  • Calculation: use stoichiometric ratios from the balanced equation to relate moles of titrant to moles of analyte.

Common Mistakes to Avoid

  1. Forgetting the acidic conditions required for permanganate and dichromate.
  2. Not balancing half-equations before combining them.
  3. Using the wrong stoichiometric ratio when calculating concentrations.
  4. Missing that permanganate is self-indicating and doesn't need an external indicator.
  5. Reading the burette at the wrong point — meniscus, eye level.

Exam Strategy

TASC Level 4 redox titration questions ask you to balance equations and calculate unknowns. Method: (1) identify the oxidising and reducing agents, (2) balance each half-equation, (3) combine to cancel electrons, (4) use stoichiometry to relate moles, (5) calculate concentration. Show each step explicitly for full marks.

Revision Tip

Redox titration calculations are procedural — drill a Revizi deck with permanganate and dichromate titrations against iron, oxalate, and hydrogen peroxide.

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Last updated: March 2026